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JIS K2436-2007 Naphthalene for industrial use.pdf

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K 2436ɿ2007 ໨ç ࣍ ϖʔδ ংจ ························································································································································································1 1ç ద༻ൣғ··········································································································································································1 2ç Ҿ༻‫··········································································································································································֨ن‬1 3ç छྨ··················································································································································································1 4ç ඼࣭··················································································································································································2 5ç ࢼ‫ํݧ‬๏··········································································································································································2 5.1ç Ұൠࣄ߲ ······································································································································································2 5.2ç ࢼྉͷ࠾औ‫ͼٴ‬ௐ੡··················································································································································2 5.3ç ‫···········································································································································································఺ݻڽ‬2 5.4ç ७౓···············································································································································································3 5.5ç ෆ७෺···········································································································································································4 5.6ç ེࢎண৭ࢼ‫ํݧ‬๏······················································································································································9 5.7ç ෆ‫ൃش‬෼ ···································································································································································· 10 5.8ç ਫ෼ଌఆํ๏ ···························································································································································· 11 6ç ‫ ················································································································································································ࠪݕ‬12 7ç දࣔ················································································································································································ 12 ෟଐॻ Aʢ‫ن‬ఆʣࢼྉ࠾औํ๏ ···································································································································· 13 ʢ1ʣ K 2436ɿ2007 ·͕͖͑ ͜ͷ‫֨ن‬͸ɼ޻‫ۀ‬ඪ४Խ๏ୈ 14 ৚ʹΑͬͯ४༻͢Δୈ 12 ৚ୈ 1 ߲ͷ‫ن‬ఆʹ‫͖ͮج‬ɼࣾஂ๏ਓ೔ຊ๕߳ ଒޻‫ۀ‬ձ(JAIA)‫ஂࡒͼٴ‬๏ਓ೔ຊ‫ڠ֨ن‬ձ(JSA)͔Βɼ޻‫ۀ‬ඪ४‫ݪ‬ҊΛ۩ͯ͠೔ຊ޻‫֨نۀ‬Λվਖ਼͢΂͖ͱ ͷਃग़͕͋Γɼ೔ຊ޻‫ۀ‬ඪ४ௐࠪձͷ৹ٞΛ‫ͯܦ‬ɼ‫ۀ࢈ࡁܦ‬େਉ͕վਖ਼ͨ͠೔ຊ޻‫͋Ͱ֨نۀ‬Δɻ ͜ΕʹΑͬͯɼJIS K 2436:1990 ͸վਖ਼͞Εɼ͜ͷ‫ʹ֨ن‬ஔ͖‫͑׵‬ΒΕͨɻ ͜ͷ‫֨ن‬͸ɼஶ࡞‫ݖ‬๏Ͱอ‫ޢ‬ର৅ͱͳ͍ͬͯΔஶ࡞෺Ͱ͋Δɻ ͜ͷ‫֨ن‬ͷҰ෦͕ɼಛ‫ݖڐ‬ɼग़‫ެئ‬։‫ޙ‬ͷಛ‫ڐ‬ग़‫ئ‬ɼ࣮༻৽Ҋ‫ݖ‬ຢ͸ग़‫ެئ‬։‫ޙ‬ͷ࣮༻৽Ҋొ࿥ग़‫ʹئ‬ ఍৮͢ΔՄೳੑ͕͋Δ͜ͱʹ஫ҙΛ‫͢ىש‬Δɻ‫ۀ࢈ࡁܦ‬େਉ‫ͼٴ‬೔ຊ޻‫ۀ‬ඪ४ௐࠪձ͸ɼ͜ͷΑ͏ͳಛ‫ڐ‬ ‫ݖ‬ɼग़‫ެئ‬։‫ޙ‬ͷಛ‫ڐ‬ग़‫ئ‬ɼ࣮༻৽Ҋ‫ݖ‬ຢ͸ग़‫ެئ‬։‫ޙ‬ͷ࣮༻৽Ҋొ࿥ग़‫܎ʹئ‬Δ֬ೝʹ͍ͭͯɼ੹೚͸ ΋ͨͳ͍ɻ ʢ2ʣ ೔ຊ޻‫֨نۀ‬ç ç ç JIS K 2436ɿ2007 ޻‫༻ۀ‬φϑλϨϯ Naphthalene for industrial use ংจ ͜ͷ‫֨ن‬͸ɼ‫͔֨نچ‬ΒɼΞϯτϥηϯ‫ͼٴ‬Χϧόκʔϧʹؔ͢Δ‫ن‬ఆΛ࡟আ͢Δͱͱ΋ʹɼՄೳͳ‫ݶ‬ ΓԽֶ੡඼‫ڞ‬௨ͷ͸Μʢ൚ʣ༻తͳࢼ‫ํݧ‬๏ʹؔ͢Δ೔ຊ޻‫֨نۀ‬ΛҾ༻͢Δ͜ͱʹΑͬͯɼ‫֨ن‬ͷॏෳ Λආ͚Δ͜ͱͳͲΛ໨తͱͯ͠վਖ਼ͨ͠ɻ ͳ͓ɼରԠࠃࡍ‫֨ن‬͸‫੍Ͱ఺࣌ݱ‬ఆ͞Ε͍ͯͳ͍ɻ 1 ద༻ൣғ ͜ͷ‫֨ن‬͸ɼ޻‫༻ۀ‬φϑλϨϯʹ͍ͭͯ‫ن‬ఆ͢Δɻ 2 Ҿ༻‫֨ن‬ ࣍ʹ‫͛ܝ‬Δ‫֨ن‬͸ɼ͜ͷ‫ʹ֨ن‬Ҿ༻͞ΕΔ͜ͱʹΑͬͯɼ͜ͷ‫֨ن‬ͷ‫ن‬ఆͷҰ෦Λߏ੒͢Δɻ͜ΕΒͷ Ҿ༻‫֨ن‬͸ɼͦͷ࠷৽൛ʢ௥ิΛ‫ؚ‬ΉɻʣΛద༻͢Δɻ JIS C 3105ç ߗಔΑΓઢ JIS K 0050ç Խֶ෼ੳํ๏௨ଇ JIS K 0068ç Խֶ੡඼ͷਫ෼ଌఆํ๏ JIS K 0114ç ΨεΫϩϚτάϥϑ෼ੳ௨ଇ JIS K 2435-1ç ϕϯθϯɾτϧΤϯɾΩγϨϯʵୈ 1 ෦ɿϕϯθϯ JIS K 8040ç Ξητϯʢ࢒ཹ೶ༀɾPCB ࢼ‫༻ݧ‬ʣʢࢼༀʣ JIS K 8125ç ԘԽΧϧγ΢Ϝʢਫ෼ଌఆ༻ʣʢࢼༀʣ JIS K 8279ç ΩϊϦϯʢࢼༀʣ JIS K 8305ç m-ΫϨκʔϧʢࢼༀʣ JIS K 8552ç ঳ࢎίόϧτʢᶘʣ࿡ਫ࿨෺ʢࢼༀʣ JIS K 8798ç ϑΣϊʔϧʢࢼༀʣ JIS K 8949ç ེԽφτϦ΢Ϝ‫۝‬ਫ࿨෺ʢࢼༀʣ JIS K 8951ç ེࢎʢࢼༀʣ JIS M 8100ç คմࠞ߹෺ʵαϯϓϦϯάํ๏௨ଇ JIS Z 8401ç ਺஋ͷ‫ؙ‬Ίํ 3 छྨ ޻‫༻ۀ‬φϑλϨϯͷछྨ͸ɼਫ਼੡φϑλϨϯ‫ ͼٴ‬95 ˋφϑλϨϯͱ͢Δɻ 2 K 2436ɿ2007 4 ඼࣭ ඼࣭͸ɼछྨʹΑͬͯ۠෼͠ɼՕ৚ 5 ʹΑͬͯࢼ‫͖ͱͨ͠ݧ‬ɼද 1 ʹΑΔɻ छྨ ߲໨ ‫఺ݻڽ‬ç ç ç ç ç ç ç ç ç ˆ ද 1ʵ඼࣭ ਫ਼੡φϑλϨϯ 79.5 Ҏ্ ७౓ç ç ç ç ç ˋʢ࣭ྔ෼཰ʣ 99 Ҏ্ ෆ७෺ ེࢎண৭ࢼ‫ݧ‬ ड౉౰ࣄऀؒͷऔܾΊʹΑΔ ൺ৭ඪ४ӷ 2 ൪ΑΓ҉͘ͳ͍ ෆ‫ൃش‬෼ç ç ç ˋʢ࣭ྔ෼཰ʣ ʵ ਫ෼ç ç ç ç ç ˋʢ࣭ྔ෼཰ʣ ʵ 95 ˋφϑλϨϯ 77.5 Ҏ্ ʢ୤ਫࢼྉʹ͖ͭʣ 95 Ҏ্ ʢ୤ਫࢼྉʹ͖ͭʣ ड౉౰ࣄऀؒͷऔܾΊʹΑΔ ʵ 0.2 ҎԼ 0.2 ҎԼ 5 ࢼ‫ํݧ‬๏ 5.1 Ұൠࣄ߲ Ұൠࣄ߲͸ɼJIS K 0050 ʹΑΔɻͨͩ͠ɼ࣍Λ௥Ճ͢Δɻ a) ୯ʹ༹ӷͱ‫͠ه‬ɼಛʹ༹ഔΛࣔ͞ͳ͍΋ͷ͸ɼਫ༹ӷΛࢦ͢ɻ b) ӷ໘Ͱ໨੝ΛಡΉͱ͖͸ɼද໘ுྗʹΑ্ͬͯঢͨ͠ӷ໘ͷԼԑͰಡΉɻ c) Թ౓‫ܭ‬͸ɼ͋Β͔͡Ίඪ४Թ౓‫ʹܭ‬Αͬͯɼߍਖ਼ͨ͠΋ͷΛ༻͍Δɻ 5.2 ࢼྉͷ࠾औ‫ͼٴ‬ௐ੡ 5.2.1 ࢼྉͷ࠾औ ࢼྉͷ࠾औํ๏͸ɼෟଐॻ A ʹΑΔɻ 5.2.2 ࢼྉͷௐ੡ ࢼྉͷௐ੡͸ɼ࣍ʹΑΔɻ a) ୅දࢼྉ໿ 100 g ΛऔΓɼೕുͰคࡅ͠ɼΑࠞͥ͘߹Θͤͯ‫ۉ‬Ұʹͨ͠΋ͷΛࢼ‫͍༻ʹݧ‬Δɻ b) a)ͷ 50 g ΛϏʔΧʔ100 mL ʹऔΓɼԹ౓໿ 85 ˆʹՃ೤ͯ͠༥ղ͢ΔɻJIS K 8125 ʹ‫ن‬ఆ͢ΔԘԽΧ ϧγ΢Ϝ 10 g ΛೖΕɼԹ౓໿ 85 ˆʹอͪͳ͕Β͠͹Β͘ͷ͔͖ؒࠞͥΔɻ5ʙ10 ෼ؒ੩ஔͨ͠‫ޙ‬ɼ ্੅ΈӷΛऔΓɼ୤ਫࢼྉͱ͢Δɻ 5.3 ‫఺ݻڽ‬ 5.3.1 ཁࢫ ࢼྉΛࢼ‫ݧ‬؅ʹऔΓɼࢼྉͷ༧૝͞ΕΔ‫఺ݻڽ‬ΑΓ௿͍Թ౓ͷਫཋதͰ੩͔ʹ͔͖ࠞͥͳ͕Βྫྷ٫͠ɼ ࢼྉ͕‫͖ͱͨ͠ݻڽ‬ͷ࠷ߴԹ౓Λଌఆ͢Δɻ 5.3.2 ਫ਼੡φϑλϨϯͷ‫఺ݻڽ‬ 5.3.2.1 ૷ஔ‫۩ثͼٴ‬ ૷ஔ‫۩ثͼٴ‬͸ɼ࣍ʹΑΔɻ a) ૷ஔç ਤ 1 ʹΑΔɻ b) ࢼ‫ݧ‬؅ç ΄͏͚͍ࢎΨϥε੡ɻ‫ܗ‬ঢ়‫ੇͼٴ‬๏͸ɼਤ 1 ʹΑΔɻ c) Թ౓‫ܭ‬ç Թ౓‫ܭ‬͸ɼJIS K 2435-1 ͷ 5.10.2 b)ͷද 9 ʹΑΔɻ d) ͔͖ࠞͥ๮ç ௚‫ܘ‬໿ 1 mm ͷ਑ۚͰɼͦͷઌ୺ͷҰํΛԁ‫ͨ͠ʹܗ‬΋ͷɻ e) େ‫ݧࢼܗ‬؅ç ‫ܗ‬ঢ়‫ੇͼٴ‬๏͸ɼਤ 1 ʹΑΔɻ f) ϏʔΧʔç ༰ྔ 1 000 mLɻਤ 1 ʹࣔ͢΋ͷɻ 3 K 2436ɿ2007 ୯Ґç mm ਤ 1ʵ‫఺ݻڽ‬ଌఆ૷ஔ 5.3.2.2 ૢ࡞ ૢ࡞͸ɼ࣍ʹΑΔɻ a) ࢼྉΛ༥ղͯ͠ӷঢ়ͱͨ͠‫ޙ‬ɼ໿ 25 mL Λࢼ‫ݧ‬؅ʹऔΓɼԹ౓ 90 ˆҎ্ͰࢼྉΛ‫׬‬શʹӷঢ়ʹอͪ ͳ͕Βɼ͜ΕʹԹ౓‫͖͔ͥࠞͼٴܭ‬๮Λࠩ͠ࠐΜͩίϧΫખΛऔΓ෇͚ΔɻԹ౓‫ܭ‬ͷਫۜ‫ٿ‬͸ɼਤ 1 ʹࣔ͢Α͏ʹɼࢼ‫ݧ‬؅಺ͷࢼྉͷதԝʹҐஔ͢ΔΑ͏ʹௐઅ͢Δɻ b) ͜Εʹ֎ͱ͏ͱͯ͠େ‫ݧࢼܗ‬؅ΛऔΓ෇͚ͨ‫ޙ‬ɼԹ౓໿ 75 ˆͷԹਫΛຬͨͨ͠ϏʔΧʔதʹࠩ͠ࠐ Έɼ2 ඵؒʹ 1 ճͷׂ߹ͰࢼྉΛ͔͖ࠞͥͳ͕Βྫྷ٫͢Δɻ c) ࢼྉ͕‫࢝͠ݻڽ‬ΊΔͱಉ࣌ʹԹ౓‫ܭ‬ͷࣔ౓্͕ঢ࢝͠Ίɼશ෦͕‫͠ݻڽ‬ऴΘΔͱԹ౓ͷ্ঢ͕ࢭ·Γɼ ࠶ͼԼ߱࢝͠ΊΔɻ͜ͷͱ͖ͷԹ౓‫ܭ‬ͷ࠷ߴࣔ౓Λ‫͢ͱ఺ݻڽ‬Δɻͨͩ͠ɼԹ౓‫ܭ‬࿐ग़෦ͷԹ౓ิਖ਼ ͸ߦΘͳ͍ɻ 5.3.3 95 ˋφϑλϨϯͷ‫఺ݻڽ‬ ୤ਫࢼྉΛ࢖༻͠ɼԹਫԹ౓͸໿ 73 ˆͱͯ͠ɼ5.3.2 ʹ‫ن‬ఆ͢Δํ๏ʹΑͬͯɼ‫఺ݻڽ‬Λଌఆ͢Δɻ 5.4 ७౓ 5.3 ʹΑͬͯଌఆͨ͠‫͔఺ݻڽ‬Βɼද 2 Λ༻͍ͯਫ਼੡φϑλϨϯ‫ ͼٴ‬95 ˋφϑλϨϯͷ७౓Λ‫ٻ‬ΊΔɻ 4 K 2436ɿ2007 ‫఺ݻڽ‬ ˆ 75.0 75.1 75.2 75.3 75.4 75.5 75.6 75.7 75.8 75.9 76.0 76.1 76.2 76.3 76.4 76.5 76.6 76.7 76.8 76.9 ද 2ʵφϑλϨϯͷ‫ͱ఺ݻڽ‬७౓ͱͷؔ܎ ७౓ ˋʢ࣭ྔ෼཰ʣ 90.0 90.2 90.4 90.6 90.8 91.0 91.2 91.4 91.6 91.8 92.0 92.2 92.4 92.6 92.8 93.0 93.2 93.4 93.6 93.8 ‫఺ݻڽ‬ ˆ 77.0 77.1 77.2 77.3 77.4 77.5 77.6 77.7 77.8 77.9 78.0 78.1 78.2 78.3 78.4 78.5 78.6 78.7 78.8 78.9 ७౓ ˋʢ࣭ྔ෼཰ʣ 94.0 94.2 94.4 94.6 94.8 95.0 95.2 95.4 95.6 95.8 96.0 96.2 96.4 96.6 96.8 97.0 97.2 97.4 97.6 97.8 ‫఺ݻڽ‬ ˆ 79.0 79.1 79.2 79.3 79.4 79.5 79.6 79.7 79.8 79.9 80.0 80.1 80.2 80.3 ७౓ ˋʢ࣭ྔ෼཰ʣ 98.0 98.2 98.4 98.6 98.8 99.0 99.2 99.4 99.5 99.6 99.7 99.8 99.9 100.0 5.5 ෆ७෺ 5.5.1 ཁࢫ ΨεΫϩϚτάϥϑ๏ʹΑͬͯɼਫ਼੡φϑλϨϯ‫ ͼٴ‬95 ˋφϑλϨϯதʹ‫·ؚ‬ΕΔෆ७෺ͷ‫ྔؚ‬Λ‫ٻ‬ ΊΔɻ ࢼ‫ڞʹݧ‬௨͢ΔҰൠࣄ߲͸ɼJIS K 0114 ʹΑΔɻ 5.5.2 ૷ஔ‫۩ثͼٴ‬ ૷ஔ‫۩ثͼٴ‬͸ɼ࣍ʹΑΔɻ a) ΨεΫϩϚτάϥϑ 1) ‫ݕ‬ग़‫ث‬ç ਫૉԌΠΦϯԽ‫ݕ‬ग़‫ث‬ɻࢼྉΛಋೖͨ͠ͱ͖ɼ௿෸఺੒෼͕े෼ʹ෼཭༹ग़͠ɼ࣭ྔ෼཰ 0.01 ˋҎ্ͷ੒෼ͷϐʔΫͷߴ͞͸ɼϊΠζϨϕϧͷ 2 ഒҎ্Ͱ͋Δ΋ͷɻ 2) ΧϥϜ༻؅ç ಺‫ ܘ‬3 mm ‫ͼٴ‬௕͞ 3 m ͷ΄͏͚͍ࢎΨϥε؅ຢ͸εςϯϨε߯؅ɻ 3) ΧϥϜç ୲ମʦ5.5.3 a) ࢀরʧʹॆͯΜࡎ༻ࢼༀʦ5.5.3 b) ࢀরʧΛ JIS K 0114 ʹ‫ن‬ఆ͢Δ୲࣋཰͕ 5 ˋʢ࣭ྔ෼཰ʣͱͳΔΑ͏ʹ୲࣋ͨ͠ॆͯΜࡎΛɼΧϥϜ༻؅ʦ5.5.2 a) 2) ࢀরʧʹॆͯΜͨ͠ ΋ͷຢ͸͜Εͱಉ౳ͷ΋ͷɻΧϥϜ͸ॆͯΜࡎΛͭΊͨࢢൢ඼Λ࢖༻͢ΔɻࣗΒॆͯΜΧϥϜΛ࡞ ੡ͯ͠ɼଌఆʹ࢖༻͢Δ৔߹ʹ͸ JIS K 0114 ͷ 7.2 e)ʢॆͯΜํ๏ʣʹΑΔɻ 4) ࢼྉಋೖ෦ç ӷମࢼྉಋೖ‫ؾͼٴޱ‬Խ‫ث‬Λඋ͑ͨ΋ͷɻ b) Խֶ͸͔Γç 0.1 mg ·Ͱ͸͔ΕΔ΋ͷɻ c) ϚΠΫϩγϦϯδç 1ʙ10 µL ͷ΋ͷɻ d) σʔλॲཧ૷ஔ 5 K 2436ɿ2007 5.5.3 ୲ମɼࢼༀ‫ͼٴ‬ΩϟϦϠʔΨε ୲ମɼࢼༀ‫ͼٴ‬ΩϟϦϠʔΨε͸ɼ࣍ʹΑΔɻ a) ୲ମç ཻ౓ 150ʙ180 µm ͷ଱ՐΕΜ͕ʢ͚͍૶౔Λओ੒෼ͱͨ͠଱ՐԹ౓ 1 100 ˆఔ౓ͷ΋ͷɻʣຢ ͸͜Εͱಉ౳ͷ΋ͷɻ ஫‫ࢢ ه‬ൢͷ୲ମʹ͸ɼϢχϙʔτɼηϥΠτ 545 ͳͲ͕͋Δɻ b) ‫ݻ‬ఆ૬ӷମç ϙϦΤεςϧʢΞϧΩϨϯάϦίʔϧϑλϧࢎΤεςϧʣ ஫‫ࢢ ه‬ൢͷॆͯΜࡎʹ͸ɼαʔϞϯ 3000 ͳͲ͕͋Δɻ c) ௐ੡༻ࢼༀ 1) Ξητϯç JIS K 8040 ʹ‫ن‬ఆ͢Δೱॖ 300 ຢ͸ಉ౳ͷ΋ͷɻ d) ‫ࢼ༻ྔݕ‬ༀç ‫ࢼ༻ྔݕ‬ༀ͸ɼ࣍ʹΑΔɻJIS ʹ‫ن‬ఆ͢Δ΋ͷҎ֎͸ɼࢼ‫ࢧʹݧ‬োͷͳ͍΋ͷΛ࢖༻͢ Δɻ 1) Πϯμϯ 2) Πϯσϯ 3) ΞητϑΣϊϯ 4) ϓϩϐΦϑΣϊϯ 5) ϕϯκνΦϑΣϯ 6) 2-ϝνϧφϑλϨϯ 7) 1-ϝνϧφϑλϨϯ 8) ΩϊϦϯʢJIS K 8279 ʹ‫ن‬ఆ͢Δ΋ͷɻʣ 9) 2,3-δϝνϧφϑλϨϯ 10) ϑΣϊʔϧʢJIS K 8798 ʹ‫ن‬ఆ͢Δ΋ͷɻʣ 11) m-ΫϨκʔϧʢJIS K 8305 ʹ‫ن‬ఆ͢Δ΋ͷɻʣ 12) 2,3-ΩγϨϊʔϧ 13) 3,5-ΩγϨϊʔϧ 14) 3,4-ΩγϨϊʔϧ 15) ϑϧΦϨϯʢ಺ඪ४෺࣭ʣ e) ΩϟϦϠʔΨεç ७౓ 99.99 ˋʢମੵ෼཰ʣҎ্ͷ஠ૉຢ͸ϔϦ΢Ϝɻ 5.5.4 ‫ྔݕ‬ ‫ྔݕ‬͸ɼ࣍ʹΑΔɻ a) ‫༻ྔݕ‬ඪ४ࢼྉͷௐ੡ç 5.5.3 d)ͷ‫ࢼ༻ྔݕ‬ༀΛ༻͍ͯɼࢼྉͷඃ‫ݕ‬੒෼ʹ͍ۙೱ౓ͷ΋ͷΛௐ੡͢Δɻ ·ͨɼ಺ඪ४෺࣭ͱͯ͠ϑϧΦϨϯΛࢼྉͷҰ൪ೱ౓ͷߴ͍ඃ‫ݕ‬੒෼ʹ߹Θͤͯௐ੡͠ɼ࣍ʹࢼྉͱ ಉҰೱ౓ʹͳΔΑ͏ʹɼΞητϯΛ༻͍ɼ‫ر‬ऍͯ͠ௐ੡͢Δɻ b) ૬ର‫౓ײ‬ͷ‫ٻ‬Ίํç 5.5.4 a)Ͱௐ੡ͨ͠‫༻ྔݕ‬ඪ४ࢼྉΛಋೖ͠ɼΫϩϚτάϥϜͷ֤ϐʔΫ໘ੵΛଌ ఆ͢ΔɻϐʔΫ໘ੵͷଌఆ͸ɼJIS K 0114 ʹΑͬͯɼσʔλॲཧ૷ஔΛ༻͍ͯߦ͍ɼϐʔΫ੒෼͝ͱ ʹ໘ੵΛࢉग़͢Δɻͨͩ͠ɼ‫ٻ‬ΊΔਫ਼౓ʹΑͬͯ͸ɼ൒஋෯๏Λ༻͍ͯ΋Α͍ɻ ֤੒෼ͷ૬ର‫౓ײ‬͸ɼ࣍ͷࣜʹΑͬͯࢉग़͠ɼJIS Z 8401 ʹΑͬͯɼখ਺఺ҎԼ 2 ͚ͨʹ‫ؙ‬ΊΔɻ ͳ͓ɼະ஌ඍྔ੒෼ͷ૬ର‫౓ײ‬͸ɼ1.00 ͱ͢Δɻ fi = Ai Wi × Ws As 6 K 2436ɿ2007 ͜͜ʹɼ fiɿ Aiɿ Wiɿ Wsɿ Asɿ i ੒෼ͷ૬ର‫౓ײ‬ i ੒෼ͷϐʔΫ໘ੵʢµVsʣ ඪ४ࢼྉதͷ i ੒෼ͷ࣭ྔʢgʣ ඪ४ࢼྉதͷ಺ඪ४෺࣭ͷ࣭ྔʢgʣ ಺ඪ४෺࣭ͷϐʔΫ໘ੵʢµVsʣ c) ૬ରอ࣋࣌ؒͷ‫ٻ‬Ίํ 1)ç 5.5.4 a)Ͱௐ੡ͨ͠‫༻ྔݕ‬ඪ४ࢼྉΛಋೖ͠ɼΫϩϚτάϥϜΛ‫ه‬࿥ͯ͠ɼ ࢼྉಋೖ࣌ʢελʔτϚʔΫʣ͔Β֤੒෼ͷϐʔΫͷ௖఺·Ͱͷ࣌ؒʢอ࣋࣌ؒʣΛ࣌ؒ໨੝ʹΑͬ ͯ 0.1 ෼ؒ·ͰಡΈऔΔɻ ֤੒෼ͷ૬ରอ࣋࣌ؒ͸ɼ࣍ͷࣜʹΑͬͯࢉग़͠ɼJIS Z 8401 ʹΑͬͯɼখ਺఺ҎԼ 2 ͚ͨʹ‫ؙ‬Ί Δɻ Ri = Ti Ts ͜͜ʹɼ Riɿ i ੒෼ͷ૬ରอ࣋࣌ؒ Tiɿ i ੒෼ͷอ࣋࣌ؒʢminʣ Tsɿ ಺ඪ४෺࣭ͷอ࣋࣌ؒʢminʣ ஫ 1) ΧϥϜɼԹ౓‫ͼٴ‬ΩϟϦϠʔΨεΛม͑ͳ͍‫ݶ‬ΓɼҰ౓ଌఆ͓͚ͯ͠͹Α͍ɻ 5.5.5 ૢ࡞ ૢ࡞͸ɼ‫ͱ࣌ྔݕ‬ಉ͡ଌఆ৚݅Ͱߦ͏ɻͨͩ͠ɼଌఆ৚݅͸‫ʹثػ‬ΑͬͯҟͳΔͷͰɼૢ࡞͸࢖༻͢Δ ‫ثػ‬ͷ࠷ద৚݅ͷ΋ͱͰߦ͏ɻ ଌఆ৚݅ͷྫΛද 3 ʹɼͦͷΫϩϚτάϥϜͷྫΛਤ 2 ʹࣔ͢ɻ 7 K 2436ɿ2007 ද 3ʵଌఆ৚݅ͷྫ ଌఆ৚݅ ࢼྉ ਫ਼੡φϑλϨϯ 95 ˋφϑλϨϯ ‫ݻ‬ఆ૬ӷମ ‫ݻ‬ఆ૬ӷମอ࣋ྔç ç ç ˋʢ࣭ྔ෼཰ʣ ୲ମʢµmʣ ΧϥϜ༻؅಺‫ͼٴܘ‬௕͞ç ç ç mmʷm ΧϥϜ૧Թ౓ç ˆʢঢԹ଎౓ç ˆ/minʣ ‫ݕ‬ग़‫ث‬Թ౓ç ç ç ç ç ç ç ç ç ˆ ࢼྉಋೖ෦Թ౓ç ç ç ç ç ç ç ˆ ϙϦΤεςϧʢΞϧΩϨϯάϦίʔϧϑλϧࢎΤ εςϧʣ 5 ଱ՐΕΜ͕ ʢ150ʙ180ʣa) 3ʷ3 160ʙ200ʢ5ʣ 240 240 ΩϟϦϠʔΨε ΩϟϦϠʔΨεྲྀྔç ç ç ç ç mL/min ஠ૉ 45 ‫ݕ‬ग़‫ث‬ ਫૉѹྗç ç ç ç ç ç ç ç ç ç kPa ۭ‫ؾ‬ѹྗç ç ç ç ç ç ç ç ç ç kPa ࢼྉಋೖྔç ç ç ç ç ç ç ç ç µL ਫૉԌΠΦϯԽ‫ݕ‬ग़‫ث‬ 58.8 49.0 1 ༹ഔ ࢼྉʗ༹ഔൺç ç ç ç ç ç ç ç g/mL Ϩϯδ ࠷খ໘ੵç ç ç ç ç ç ç ç ç ç µVs Ξςωʔγϣϯ ‫ه‬࿥ࢴૹΓ଎౓ç ç ç ç ç ç ç mm/min Ξητϯ 10/30 103 100 22 10 ‫ํࢉܭ‬๏ શ໘ੵç ç ç ç ç ç ç ç ç ç ç µVs ಺ඪ४๏ 10 000 000 ஫ a) ཻ౓ 150ʙ180 µm ͷ଱ՐΕΜ͕ʢ͚͍૶౔Λओ੒෼ͱͨ͠଱ՐԹ౓ 1 100 ˆఔ౓ͷ΋ ͷɻʣຢ͸͜Εͱಉ౳ͷ΋ͷɻ 8 K 2436ɿ2007 ਤ 2ʵΨεΫϩϚτάϥϜͷྫ 5.5.6 ‫ࢉܭ‬ ෆ७෺ͷ‫ྔؚ‬͸ɼ࣍ͷࣜʹΑͬͯࢉग़͠ɼJIS Z 8401 ʹΑͬͯɼখ਺఺ҎԼ 1 ͚ͨʹ‫ؙ‬ΊΔɻ Ci = Ai × Ws ×100 fi × As S 9 K 2436ɿ2007 ͜͜ʹɼ 5.6 ེࢎண৭ࢼ‫ํݧ‬๏ 5.6.1 ཁࢫ Ciɿ Aiɿ fiɿ Asɿ Wsɿ Sɿ i ੒෼ͷ‫ྔؚ‬ç %ʢ࣭ྔ෼཰ʣ i ੒෼ͷϐʔΫ໘ੵʢµVsʣ i ੒෼ͷ૬ର‫౓ײ‬ ಺ඪ४෺࣭ͷϐʔΫ໘ੵʢµVsʣ ಺ඪ४෺࣭ͷ࣭ྔʢgʣ ࢼྉͷ࣭ྔʢgʣ ེࢎதʹࢼྉΛՃ͑ɼΑ͘ৼΓࠞͥͨ‫ޙ‬ɼ௚ͪʹེࢎ૚ͷண৭౓Λൺ৭ඪ४ӷͱൺ৭͢Δɻ 5.6.2 ‫۩ث‬ ‫۩ث‬͸ɼ࣍ʹΑΔɻ a) ࢼ‫ݧ‬؅ç ಺‫ ܘ‬27ʶ1 mmɼ௕͞ 120ʶ3 mm ͷ΋ͷɻ b) ࡾ֯ϑϥείç ༰ྔ 200 mL ͷ΋ͷɻ c) γϦϯδç 0.2 mL Λ͸͔ΓऔΕΔ΋ͷɻ d) ਫཋç 80ʶ1 ˆʹௐઅͰ͖Δ΋ͷɻ 5.6.3 ࢼༀ ࢼༀ͸ɼ࣍ʹΑΔɻ a) ঳ࢎίόϧτʢᶘʣ࿡ਫ࿨෺ç JIS K 8552 ʹ‫ن‬ఆ͢Δ΋ͷɻ b) ེԽφτϦ΢Ϝ‫۝‬ਫ࿨෺ç JIS K 8949 ʹ‫ن‬ఆ͢Δ΋ͷɻ c) ེࢎç JIS K 8951 ʹ‫ن‬ఆ͢Δ΋ͷɻ 5.6.4 ൺ৭ඪ४ӷͷௐ੡ ঳ࢎίόϧτʢᶘʣ࿡ਫ࿨෺ 5 g Λࡾ֯ϑϥείʹ͸͔ΓऔΓɼਫ 100 mL ΛՃ༹͔͑ͯͨ͠΋ͷΛ঳ࢎ ίόϧτ༹ӷͱ͢Δɻ ·ͨɼེԽφτϦ΢Ϝ‫۝‬ਫ࿨෺ 0.1 g Λࡾ֯ϑϥείʹ͸͔ΓऔΓɼਫ 100 mL ΛՃ༹͔͑ͯͨ͠΋ͷΛ ེԽφτϦ΢Ϝ༹ӷͱ͢Δɻද 4 ʹࣔࠞ͢߹ׂ߹ʹΑͬͯൺ৭ඪ४ӷΛௐ੡͢ΔɻེԽφτϦ΢Ϝ༹ӷ 0.2 mL ΛՃ͑Δͱ͖͸ɼγϦϯδΛ༻͍Δɻ ൺ৭ඪ४ӷ͸ɼࢼ‫ݧ‬ͷ౎౓ௐ੡͢Δɻ ൺ৭ඪ४ӷ 1൪ 2൪ 3൪ ද 4ʵൺ৭ඪ४ӷͷௐ੡ද ঳ࢎίόϧτ༹ӷ 2 6 10 ࠞ߹ׂ߹ ਫ 10 10 ʵ ୯Ґç mL ེԽφτϦ΢Ϝ༹ӷ 0.2 0.2 0.2 5.6.5 ૢ࡞ ེࢎ 10 mL Λࢼ‫ݧ‬؅ʹ͸͔ΓऔΓɼਫཋ্Ͱ 80 ˆʹՃ೤͢Δɻ͜ͷதʹคࡅͨ͠ࢼྉ 2 g ΛೖΕɼਖ਼ ֬ʹ 2 ෼ؒ؇΍͔ʹৼΓಈ͔ͨ͠‫ޙ‬ɼ௚ͪʹེࢎ૚ͷண৭౓Λɼଞͷࢼ‫ݧ‬؅ʹೖΕͨൺ৭ඪ४ӷͱɼഎ‫ޙ‬ ʹനࢴΛஔ͍ͯͦΕͧΕ؅ͷଆ໘͔Βಁ͔ͯ͠‫ͯݟ‬ൺ৭͢Δɻ 10 K 2436ɿ2007 5.7 ෆ‫ൃش‬෼ 5.7.1 ཁࢫ ࢼྉΛՃ೤ཋதͰۭ‫ؾ‬Λ௨͠ͳ͕ΒՃ೤ͯ͠ɼφϑλϨϯΛ‫ͤ͞ൃش‬ɼ࢒෼͸ߋʹ‫ס‬૩࣭ͯ͠ྔΛ͸͔ Δɻ͜ͷૢ࡞͸ɼυϥϑτ಺Ͱߦ͏͜ͱ͕๬·͍͠ɻ 5.7.2 ૷ஔ‫۩ثͼٴ‬ ૷ஔ‫۩ثͼٴ‬͸ɼ࣍ʹΑΔɻ a) ૷ஔç ૷ஔ͸ɼਤ 3 ʹࣔ͢ྫͷΑ͏ʹ૊ΈཱͯΔɻ b) ৠൃ‫ث‬ç ࣭ྔ 40 g ҎԼͷΨϥε੡༰‫͠ͱث‬ɼ‫ܗ‬ঢ়‫ੇͼٴ‬๏͸ਤ 4 ʹΑΔɻ c) Ճ೤ཋç Թ౓ 150ʶ5 ˆʹՃ೤‫ͼٴ‬ௐઅͰ͖ΔάϦηϦϯɼγϦίʔϯΦΠϧͳͲΛ༻͍ͨ΋ͷɻ d) ۭ‫ૹؾ‬ೖઃඋç ຖ෼໿ 3 L ͷۭ‫ؾ‬ΛఆৗతʹૹೖͰ͖Δ΋ͷɻ e) ‫ס‬૩‫ث‬ç Թ౓Λ໿ 110ʶ5 ˆʹอͯΔ΋ͷɻ f) Խֶ͸͔Γç 0.1 mg ·Ͱ͸͔ΕΔ΋ͷɻ g) σγέʔλʔ ਤ 3ʵෆ‫ൃش‬෼ଌఆ૷ஔͷྫ ୯Ґç mm 11 K 2436ɿ2007 ਤ 4ʵෆ‫ൃش‬෼ଌఆ༻ৠൃ‫ث‬ 5.7.3 ૢ࡞ ૢ࡞͸ɼ࣍ʹΑΔɻ a) શ૷ஔΛਤ 3 ͷΑ͏ʹ૊ΈཱͯΔɻ b) ͋Β͔͡Ί 150ʶ5 ˆͰ߃ྔͱͨ͠ৠൃ‫ث‬ͷ࣭ྔΛ 1 mg ·Ͱ͸͔Γɼ͜Εʹࢼྉ໿ 10 g Λ 1 mg ·Ͱ ͸͔ΓऔΓɼ150ʶ5 ˆʹՃ೤ͨ͠άϦηϦϯͳͲͷՃ೤ཋதʹͰ͖Δ͚ͩਂ͘ਁ͠ɼۭ‫ؾ‬Λຖ෼໿ 3 L ͷׂ߹Ͱ 30 ෼ؒ௨ͯ͠φϑλϨϯΛ‫ͤ͞ൃش‬Δɻ c) ৠൃ‫ث‬ΛՃ೤ཋ͔ΒऔΓग़͠ɼͦͷ֎෦Λચͬͨ‫ޙ‬ɼ110ʶ5 ˆͷ‫ס‬૩‫ث‬தͰ߃ྔʹͳΔ·Ͱ‫ס‬૩ͤ͞ɼ σγέʔλʔதͰ໿ 90 ෼ؒ์ྫྷͨ͠‫ޙ‬ɼ࣭ྔΛ͸͔Δɻ͜ͷૢ࡞Λ‫܁‬Γฦͯ͠߃ྔͱ͢Δɻ ஫‫ ه‬c)ͷ‫ס‬૩͸ɼ௨ৗ໿ 2 ࣌ؒͰ߃ྔʹͳΔɻ 5.7.4 ‫ࢉܭ‬ ෆ‫ൃش‬෼͸ɼ࣍ͷࣜʹΑͬͯࢉग़͠ɼJIS Z 8401 ʹΑͬͯɼখ਺఺ҎԼ 1 ͚ͨʹ‫ؙ‬ΊΔɻ N = A − B ×100 S 5.8 ਫ෼ଌఆํ๏ 5.8.1 ཁࢫ ͜͜ʹɼ Nɿ ෆ‫ൃش‬෼ʢˋʣʢ࣭ྔ෼཰ʣ Aɿ ৠൃ‫࢒ͼٴث‬෼ͷ࣭ྔʢgʣ Bɿ ৠൃ‫ث‬ͷ࣭ྔʢgʣ Sɿ ࢼྉͷ࣭ྔʢgʣ ਫ෼ଌఆ͸ɼJIS K 0068 ͷ 6.3 ʹ‫ن‬ఆ͢ΔΧʔϧϑΟογϟʔ༰ྔణఆ๏ຢ͸ JIS K 0068 ͷ 6.4 ʹ‫ن‬ఆ ͢ΔΧʔϧϑΟογϟʔిྔణఆ๏ͷ͍ͣΕ͔ʹΑͬͯߦ͏ɻ 12 K 2436ɿ2007 5.8.2 ࢼༀ ࢼༀ͸ɼJIS K 0068 ͷ 6.3.3ʢࢼༀʣຢ͸ 6.4.3ʢࢼༀʣʹΑΔɻ 5.8.3 ૷ஔ ૷ஔ͸ɼJIS K 0068 ͷ 6.3.2ʢ૷ஔ‫۩ثͼٴ‬ʣຢ͸ 6.4.2ʢ૷ஔ‫۩ثͼٴ‬ʣʹΑΔɻ 5.8.4 ࢼྉͷྔ ࢼྉͷྔ͸ɼJIS K 0068 ͷ 6.2ʢࢼྉͷ࠾औʣʹΑΔɻ 5.8.5 ૢ࡞ ૢ࡞͸ɼJIS K 0068 ͷ 6.3.4ʢࢼྉ࠾औૢ࡞ʣɼ‫ ͼٴ‬6.3.5ʢૢ࡞ʣຢ͸ 6.4.4ʢૢ࡞ʣʹΑΔɻ ஫‫ ه‬1 ࢼྉ࠾औ༰‫ث‬͸ɼJIS K 0068 ͷਤ 7 ʹྫࣔ͞Ε͍ͯΔ஫ࣹ౵‫ݻܗ‬ମࢼྉ࠾औ‫ث‬Λ࢖༻͢Δͱ ࢼྉ࠾औ͕༰қͰ͋Δɻ ஫‫ ه‬2 ణఆ༹ࡎ͸ɼJIS K 0068 ͷ 6.3.3 j) 2)ʢϝλϊʔϧʵΫϩϩϗϧϜࠞ߹༹ഔʣʹ‫͞ࡌه‬Ε͍ͯ ΔϝλϊʔϧʵΫϩϩϗϧϜࠞ߹༹ࡎΛ༻͍Δ͜ͱ͕ద੾Ͱ͋Δɻ 5.8.6 ‫ํࢉܭ‬๏ ‫ํࢉܭ‬๏͸ɼJIS K 0068 ͷ 6.3.6ʢ‫ࢉܭ‬ʣຢ͸ 6.4.5ʢ‫ࢉܭ‬ʣʹΑΔɻ 6 ‫ࠪݕ‬ ‫ࠪݕ‬͸ɼՕ৚ 5 ʹΑͬͯࢼ‫͠ݧ‬ɼද 1 ʹద߹͠ͳ͚Ε͹ͳΒͳ͍ɻ 7 දࣔ φϑλϨϯͷ༰‫ʹث‬͸ɼ࣍ͷࣄ߲Λදࣔ͠ͳ͚Ε͹ͳΒͳ͍ɻͨͩ͠ɼେ‫ܗ‬༰‫ث‬ʢλϯΫϩʔϦʔɼ՟ ंͳͲʣͷ৔߹ʹ͸ɼૹΓঢ়ʹදࣔͯ͠΋Α͍ɻ a) ‫֨ن‬൪߸‫ͼٴ‬छྨ b) ਖ਼ຯ࣭ྔຢ͸ਖ਼ຯ༰ྔ c) ੡଄೥݄ຢ͸ͦͷུ߸ d) ੡଄൪߸ e) ੡଄‫໊ऀۀ‬ຢ͸ͦͷུ߸ ෟଐॻ A ʢ‫ن‬ఆʣ ࢼྉ࠾औํ๏ 13 K 2436ɿ2007 ংจ ͜ͷෟଐॻ͸ɼࢼྉ࠾औํ๏ʹ͍ͭͯ‫ن‬ఆ͢Δɻ A.1 Ұൠࣄ߲ A.1.1 Ұൠ A.1.1.1 ࢼྉͷ࠾औ͸ɼࡏ‫ݿ‬඼ɼੵՙɼҠૹதͷύΠϓϥΠϯͳͲ͔Βߦ͏ɻ A.1.1.2 ๕߳଒੡඼‫ͼٴ‬λʔϧ੡඼͸ɼߴҾՐੑͷ‫ݥة‬෺‫ͼٴ‬༗֐ੑͷ੡඼͕ଟ͍ͷͰɼͦͷऔѻ͍ʹ͸ ઃඋ্‫े্࡞ૢͼٴ‬෼ͳ஫ҙ͕ඞཁͰ͋Δɻ A.1.2 ༰‫ث‬ͷछผ A.1.2.1 ӷମ੡඼‫ͼٴ‬൒‫ݻ‬ମ੡඼ͷ৔߹ a) খ‫ܗ‬༰‫ث‬ç 18 L ؈ɼυϥϜ؈ͳͲ b) େ‫ܗ‬༰‫ث‬ç λϯΫɼλϯΧʔɼλϯΫंɼλϯΫϩʔϦʔͳͲ A.1.2.2 ‫ݻ‬ମ੡඼ͷ৔߹ a) খ‫ܗ‬༰‫ث‬ç ାɼυϥϜ؈ͳͲ b) େ‫ܗ‬༰‫ث‬ç αΠϩɼધɼ՟ंɼτϥοΫɼ͹ΒੵΈͳͲ A.1.3 ༻‫ޠ‬ͷఆٛ ༻‫ޠ‬ͷఆٛ͸ɼ࣍ʹΑΔɻ a) ϩοτç ϩοτͱ͸ɼಉҰͷ؅ཧ৚݅Լʹੜ࢈‫ͼٴ‬ஷଂ͞ΕɼಉҰͷ඼࣭ͱ‫ͯ͠ͳݟ‬ɼಉ͡औѻ͍Λ ͢Δ੡඼ͷू·Γɻ b) ୅දࢼྉç 1 ϩοτͷ੡඼ͷฏ‫ۉ‬඼࣭Λ୅ද͢ΔΑ͏ʹ࠾औͨ͠ࢼྉɻ A.1.4 ϩοτͷࣝผ 1 ϩοτͷ੡඼Λখ‫ܗ‬༰‫ʹث‬ೖΕΔͱ͖͸ɼ༰‫ʹͱ͝ث‬੡඼໊ɼ੡଄ॴ໊ɼॆͯΜ೥݄೔ɼϩοτ൪߸ ͳͲΛ‫͢ࡌه‬Δɻ A.1.5 ࢼྉͷ࠾औͷ࣌‫ͼٴظ‬৔ॴ ࢼྉ࠾औͷ࣌‫ͼٴظ‬৔ॴ͸ɼड౉౰ࣄऀؒͷ‫ڠ‬ٞʹΑΔɻ ͳ͓ɼߴҾՐੑͷϕϯθϯɼτϧΤϯͳͲΛλϯΫ্෦͔Β࠾औ͢Δํ๏͸ɼ҆શରࡦ্໰୊͕ଟ͍ͷ ͰɼͰ͖Δ͚ͩλϯΫɼύΠϓϥΠϯͳͲͷϊζϧ͔Β࠾औ͢Δɻ A.1.6 ༰‫ث‬ͷൈऔ‫਺ݸ‬ ෳ਺ͷ༰‫͔ث‬ΒͳΔϩοτͷ୅දࢼྉΛ࠾औ͢Δͱ͖͸ɼද A.1 ຢ͸ද A.2 ʹࣔ͢‫਺ݸ‬ͷ༰‫ث‬Λϥϯμ Ϝʹൈ͖औΓɼͦΕͧΕ 1 ‫ݸ‬ͷࢼྉΛ࠾औͯ͠ಉྔͣͭࠞ߹ͨ͠΋ͷΛ୅දࢼྉͱ͢Δɻͨͩ͠ɼେ‫ܗ‬༰ ‫͍͓ͯʹͲͳث‬ɼ಺༰ྔ͕ͦΕͧΕҟͳΔͱ͖͸ɼ΄΅಺༰ྔʹൺྫ͢ΔࢼྉྔΛࠞ߹ͯ͠୅දࢼྉͱ͢ Δɻ 14 K 2436ɿ2007 ද A.1ʵൈऔ‫਺ݸ‬ʢϩοτ൪߸͕໌ࣔ͞Ε͍ͯΔ৔߹ʣ ༰‫਺ث‬ 1ʙ 3 4ʙ 64 65ʙ125 ൈऔ‫਺ݸ‬ ʢ࠷௿ʣ શ਺ 4 5 ༰‫਺ث‬ 126ʙ216 217ʙ343 344ʙ512 ൈऔ‫਺ݸ‬ ʢ࠷௿ʣ 6 7 8 දʹࣔͨ͠༰‫਺ث‬Ҏ্ͷ৔߹͸ɼ༰‫਺ث‬ͷཱํࠜʢ੾Γ্͛ͨ ੔਺ʣΛൈऔ‫͢ͱ਺ݸ‬Δɻ ஫‫ ه‬༰‫ ਺ث‬64 Ҏ্ͷൈऔ‫਺ݸ‬͸ɼ༰‫਺ث‬ͷཱํࠜʢ੾Γ্͛ͨ ੔਺ʣʹ‫͍ͨͮج‬΋ͷͰ͋Δɻ ද A.2ʵൈऔ‫਺ݸ‬ʢϩοτ൪߸͕ෆ໌ͷ৔߹ʣ ༰‫਺ث‬ ൈऔ‫਺ݸ‬ ༰‫਺ث‬ ൈऔ‫਺ݸ‬ 1ʙ 10 11ʙ 49 50ʙ 64 65ʙ 81 82ʙ101 102ʙ125 126ʙ151 152ʙ181 ʢ࠷௿ʣ શ਺ 11 12 13 14 15 16 17 182ʙ216 217ʙ254 255ʙ296 297ʙ343 344ʙ394 395ʙ450 451ʙ512 ʢ࠷௿ʣ 18 19 20 21 22 23 24 දʹࣔͨ͠༰‫਺ث‬Ҏ্ͷ৔߹͸ɼ༰‫਺ث‬ͷཱํࠜͷ 3 ഒʢ੾Γ ্͛ͨ੔਺ʣΛൈऔ‫͢ͱ਺ݸ‬Δɻ ஫‫͜ ه‬ͷදͷൈऔ‫਺ݸ‬͸ɼ༰‫਺ث‬ͷཱํࠜͷ 3 ഒʢ੾Γ্͛ͨ ੔਺ʣʹ‫͍ͨͮج‬΋ͷͰ͋Δɻ A.1.7 ࢼྉΛ࠾औͨ͠ࢼྉ༰‫ʹث‬͸ɼࢼྉͷ໊শɼ࠾औ೥݄೔ɼ੡଄‫໊ऀۀ‬ɼϩοτ൪߸ͳͲɼඞཁࣄ߲ Λ‫ه‬ೖͨ͠ࡳͳͲΛऔΓ෇͚Δɻ A.2 ӷମࢼྉ࠾औํ๏ A.2.1 ૷ஔ‫۩ثͼٴ‬ A.2.1.1 A.2.1.2 A.2.1.3 খ‫ܗ‬ӷମࢼྉ࠾औ‫ث‬ç ྫΛਤ A.1 ʹࣔ͢ɻ େ‫ܗ‬ӷମࢼྉ࠾औ‫ث‬ç ྫΛਤ A.2 ʹࣔ͢ɻç λϯΫࢼྉ࠾औ༻ϊζϧ 1)ç ྫΛਤ A.3 ʹࣔ͢ɻ λϯΫࢼྉ࠾औ༻ϊζϧ͸ɼλϯΫͷߴ͞ʹԊͬͯ౳ִؒʹগͳ͘ͱ΋ 3 ‫ݸ‬ઃ͚Δɻ ஫ 1) ϊζϧͷλϯΫ಺෦෼ͷઌ୺͸ɼӷ໘ͱͷ੩ి‫ి์ؾ‬ͷ‫ݥة‬Λ๷ࢭ͢ΔͨΊͷे෼ͳରࡦ͕ඞ ཁͰ͋Δɻ A.2.1.4 ύΠϓϥΠϯࢼྉ࠾औ༻ϊζϧç ྫΛਤ A.4 ʹࣔ͢ɻ A.2.1.5 ີดࣜύΠϓϥΠϯࢼྉ࠾औ૷ஔç ࢼྉΛ࠾औ͢ΔϓϩηεύΠϓϥΠϯʹόΠύεΛઃ͚ɼό Πύεͷதؒʹ༰қʹ୤ணՄೳͳ‫ܧ‬खʹΑͬͯࢼྉ࠾औ༻ϘϯϕΛऔΓ෇͚ΒΕΔΑ͏ʹͨ͠΋ͷɻόΠ ύεϥΠϯʹ͸ɼྲྀग़Λ๷ࢭ͢ΔͨΊͷดࢭหΛ্Լྲྀʹઃ͚Δɻ૷ஔͷྫΛਤ A.5 ʹࣔ͢ɻ ͳ͓ɼີดࣜύΠϓϥΠϯࢼྉ࠾औ૷ஔ͸ɼ͢΂ͯ૷ஔͷ‫ݐ‬ઃɾӡసʹ܎Δ๏‫ن‬ɾ‫ج‬४ʹద߹͢Δͱͱ 15 K 2436ɿ2007 ΋ʹɼϓϩηεύΠϓϥΠϯͷ࠷ߴ࢖༻ѹྗͷ 1.5 ഒҎ্ͷѹྗʹ଱͑Δ΋ͷͱ͢Δɻ A.2.1.6 ࢼྉ༰‫ث‬ç ੡඼ͱ൓Ԡͤͣɼ੒෼͕੡඼தʹ༹ग़͠ͳ͍ࡐ࣭ͷ΋ͷͰɼີખͰ͖Δ΋ͷɻ ͳ͓ɼλʔϧԘ‫Ͳͳྨج‬ͷΑ͏ʹɼޫʹΑͬͯมԽ͠΍͍͢ࢼྉͷͱ͖͸ɼःޫੑͷ΋ͷΛ༻͍Δɻ ୯Ґç mm ਤ A.1ʵখ‫ܗ‬ӷମࢼྉ࠾औ‫ث‬ͷྫ 16 K 2436ɿ2007 ୯Ґç mm ʢ͓΋Γ෇͖ۚଐ੡࠾औ‫ث‬ʣ ඼໊ ֤෦ͷੇ๏‫߸ه‬ 260mLʢࡉ‫ޱ‬ʣ 500mLʢࡉ‫ޱ‬ʣ 500mLʢ޿‫ޱ‬ʣ 1Lʢࡉ‫ޱ‬ʣ 1Lʢ޿‫ޱ‬ʣ A 20ʶ1 20ʶ1 40ʶ1 20ʶ1 40ʶ1 B 45ʶ1 55ʶ1 55ʶ1 76ʶ1 76ʶ1 C 51ʶ2 61ʶ2 61ʶ2 82ʶ2 82ʶ2 D 50ʶ3 45ʶ3 45ʶ3 45ʶ3 45ʶ3 E 15ʶ2 20ʶ2 20ʶ2 25ʶ2 25ʶ2 F 40ʶ3 55ʶ3 55ʶ3 70ʶ3 70ʶ3 G 60ʶ3 80ʶ3 80ʶ3 100ʶ3 100ʶ3 H 155ʶ3 220ʶ3 220ʶ3 255ʶ3 255ʶ3 I 260ʶ10 340ʶ10 340ʶ10 395ʶ10 395ʶ10 ஫ a) ԫಔ੡࠾औ‫ث‬Λ࢖༻͢Δͱࢼྉ͕Ԛછ͢Δ͓ͦΕ͕͋Δ৔߹͸ɼεςϯϨε߯੡࠾औ‫ث‬Λ༻͍ͯ΋Α͍ɻ ͨͩ͠ɼεςϯϨε߯͸ SUS304 ૬౰඼Ͱɼఈ൘ͷް͞ 15 mm ͷ΋ͷͱ͢Δɻ ͳ͓ɼ͜ͷ৔߹͸ɼԼ෦ͷ͓΋ΓʢԖ੡ʣ͸͍Βͳ͍ɻ b) JIS C 3105 ʹ‫ن‬ఆ͢Δಔ੡ΑΓઢͰɼ຤୺ʹΞʔε༻ΫϥϯϓΛऔΓ෇͚Δɻ c) ʢχʣ‫ͼٴ‬ʢϗʣ͸ɼ༰қʹ཭Εͳ͍Α͏ʹ઀ଓͨ͠‫ޙ‬ɼͦΕͧΕΖ͏෇͚͢Δɻ ਤ A.2ʵେ‫ܗ‬ӷମࢼྉ࠾औ‫ث‬ͷྫ ୯Ґç mm 17 K 2436ɿ2007 ஫ a)ç A.2.2.2b)ͷ஫ 2)ࢀরɻ ਤ A.3ʵλϯΫࢼྉ࠾औ༻ϊζϧͷྫ ਤ A.4ʵύΠϓϥΠϯࢼྉ࠾औ༻ϊζϧͷྫ 18 K 2436ɿ2007 ਤ A.5ʵີดࣜύΠϓϥΠϯࢼྉ࠾औ૷ஔͷྫ A.2.2 ૢ࡞ A.2.2.1 খ‫ܗ‬༰‫ث‬ͷ৔߹ খ‫ܗ‬ӷମࢼྉ࠾औ‫ث‬ͷ‫ޱ‬Λ։͍ͨ··༰‫ʹ಺ث‬ਨ௚ʹೖΕɼ‫ث‬ఈʹୡͨ͠‫ޙ‬ɼ্෦ͷ‫ޱ‬ΛखͰดͯ͡औ Γग़͠ɼ࠾औͨ͠ࢼྉΛࢼྉ༰‫ʹث‬Ҡ͠ೖΕͯີખ͢Δɻ A.2.2.2 େ‫ܗ‬༰‫ث‬ͷ৔߹ େ‫ܗ‬༰‫ث‬ͷ৔߹͸ɼ࣍ʹΑΔɻ a) େ‫ܗ‬ӷମࢼྉ࠾औ‫ث‬Λ༻͍ͯ࠾औ͢Δ৔߹ç λϯΫͷ;ͨΛ։͖ɼΞʔεͨ͠େ‫ܗ‬ӷମࢼྉ࠾औ‫ث‬Λ ‫ޱ‬Λดͨ͡··λϯΫ಺ʹਨ௚ʹೖΕɼ࠾औ‫ث‬ͷ‫ॴ͕ޱ‬ఆͷ࠾औҐஔʹୡͨ͠ͱ͖͜ΕΛ։͍ͯࢼྉ Λྲྀ͠ࠐΈɼͦͷ··औΓग़͠ɼద੾ͳࢼྉ༰‫ʹث‬த਎ΛҠ͠ɼખΛ͢Δɻ࠾औͨ͠ࢼྉ͸ɼࢼ‫ࣨݧ‬ Ͱॴఆͷࠞ߹ׂ߹Ͱࠞ߹ͯ͠୅දࢼྉͱ͢Δɻ ࢼྉͷ࠾औҐஔ‫ࢼͼٴ‬ྉͷࠞ߹ׂ߹͸ɼԣஔԁ౵‫ܗ‬λϯΫͷ৔߹͸ද A.3 ʹΑΔɻͦͷଞͷλϯΫ ͷ৔߹͸ɼ಺༰෺Λ͓͓Αͦ 3 ౳෼֤ͨ͠૚ͷத৺෦͔Β࠾औ͠ɼͦΕͧΕ౳ྔͣͭࠞ߹͢Δɻ 19 K 2436ɿ2007 ද A.3ʵԣஔԁ౵‫ܗ‬λϯΫͷࢼྉͷ࠾औҐஔ‫ࢼͼٴ‬ྉͷࠞ߹ׂ߹ ಺༰෺ͷਂ͞ ʢ௚‫ʹܘ‬ର͢Δˋʣ 100 90 80 70 60 50 40 30 20 10 ࠾औҐஔʢఈ͔Βͷߴ͞ʣ ʢ௚‫ʹܘ‬ର͢Δˋʣ ্෦ 80 75 70 ʵ ʵ ʵ ʵ ʵ ʵ ʵ த෦ 50 50 50 50 50 40 ʵ ʵ ʵ ʵ Լ෦ 20 20 20 20 20 20 20 15 10 5 ࠞ߹ׂ߹ʢମੵʣ ্෦ 3 3 2 ʵ ʵ ʵ ʵ ʵ ʵ ʵ த෦ 4 4 5 6 5 4 ʵ ʵ ʵ ʵ Լ෦ 3 3 3 4 5 6 10 10 10 10 b) λϯΫࢼྉ࠾औ༻ϊζϧ͔Β࠾औ͢Δ৔߹ç ࢼྉͷ࠾औʹઌཱͪɼϊζϧ͔ΒλϯΫͷ಺༰෺Λྲྀग़ ͤͯ͞ࢼྉͷ௨࿏Λे෼ʹચ͍ɼ࣍ʹɼਗ਼ড়ͳ஫ೖ؅ 2)Λϊζϧʹ࿈݁͢Δɻ஫ೖ؅ͷྫΛਤ A.3 ʹ ࣔ͢ɻ ࣍ʹɼத෦ɼԼ෦‫্ͼٴ‬෦ͷ֤λοϓ͔ΒͦΕͧΕࢼྉΛ࠾औ͢Δɻࢼྉ༰‫ࢼʹث‬ྉΛຬͨͨ͠‫ޙ‬ɼ ࢼ‫ࢼͰࣨݧ‬ྉ༰‫͔ث‬Β౳ྔͣͭࢼྉΛऔͬͯࠞ߹͠ɼ୅දࢼྉͱ͢Δɻ ஫ 2) ࢼྉ༰‫ࠐࠩ͠ʹ಺ث‬ΜͰɼࢼྉΛ஫ೖ͢ΔͨΊͷ஫ೖ؅Ͱ͋ΔɻࢼྉΛ࠾औ͢Δͱ͖ɼ੡඼Λ Ԛછͨ͠ΓѱӨ‫ڹ‬Λ༩͑ͨΓ͠ͳ͍΋ͷͰɼఈ·Ͱಧ͘௕͕͞ͳ͚Ε͹ͳΒͳ͍ɻ A.2.2.3 ҠૹதͷύΠϓϥΠϯ͔Β࠾औ͢Δ৔߹ ύΠϓϥΠϯʹΑͬͯҠૹ͢Δϩοτʹ͓͍ͯ͸ɼશҠૹ࣌ؒΛ౳෼͢Δதؒ࣌఺ʹ͓͍ͯɼ3 ճҎ্ ࢼྉΛ࠾औ͠ɼͦΕͧΕ౳ྔʹࠞ߹ͯ͠୅දࢼྉͱ͢Δɻ ૢ࡞͸ɼͦΕͧΕ࣍ʹΑΔɻ a) ύΠϓϥΠϯࢼྉ࠾औ༻ϊζϧʹΑΔࢼྉ࠾औç ࢼྉ࠾औʹઌཱͪɼίοΫΛ։͍ͯ಺༰෺Λྲྀग़͞ ͤͯɼࢼྉͷ௨࿏Λे෼ʹચͬͨ‫ޙ‬ɼࢼྉ༰‫ࢼʹث‬ྉΛঃʑʹྲྀ͠ೖΕͯ࠾औ͢Δɻ b) ີดࣜύΠϓϥΠϯࢼྉ࠾औ૷ஔʹΑΔࢼྉ࠾औç ີดࣜύΠϓϥΠϯࢼྉ࠾औ૷ஔʹΑΔࢼྉ࠾ औ͸ɼ࣍ʹΑΔɻ 1) ਤ A.5 ʹ͓͍ͯɼดࢭห A ‫ͼٴ‬ดࢭห F ͸ඞཁͳͱ͖Ҏ֎͸։͍͓͖ͯɼดࢭห Bɼดࢭห E ‫ͼٴ‬ ͦͷؒͷυϨϯหΛดΊ͓͖ͯɼࢼྉ࠾औΛߦ͏ͱ͖͸ࢼྉ࠾औ༻ϘϯϕʢҎԼɼϘϯϕͱ͍͏ɻʣ Λ 2 ͔ॴͷ݁߹‫ܧ‬खʹΑͬͯਤ A.5 ͷΑ͏ʹऔΓ෇͚Δɻ 2) Ϙϯϕͷดࢭห C ‫ͼٴ‬ดࢭห D ͸ดΊ͓͖ͯɼดࢭห B Λগ͠։͖ߋʹυϨϯหΛ։͍ͯগྔͷ ӷΛྲྀͯͦ͠ͷ಺෦Λਗ਼ড়ʹ͢Δɻ࣍ʹɼดࢭห C ‫ͼٴ‬ดࢭห D Λ։͖υϨϯห͔ΒগྔͷӷΛྲྀ ͯͦ͠ͷ಺෦Λਗ਼ড়ʹ͢Δɻଓ͍ͯดࢭห E Λগ͠։͖ɼࣗಈࠩѹௐ੔ห‫ྔྲྀͼٴ‬ௐઅࢦࣔ‫ʹܭ‬Α ͬͯྲྀྔΛௐઅ͠ɼϘϯϕͷ಺෦͕े෼ʹϓϩηεύΠϓϥΠϯதͷӷʹஔ͖‫׵‬ΘΔΑ͏ʹྲྀ͠ଓ ͚Δɻ 3) όΠύεϥΠϯͷดࢭห Bɼ‫ͼٴ‬ดࢭห E ΛดΊΔͱͱ΋ʹɼϘϯϕͷग़ೖ‫ޱ‬ͷดࢭห Cɼ‫ͼٴ‬ด ࢭห D ΛดΊΔɻ 4) ֤υϨϯหΛগ͠։͍֤ͯดࢭหͷ࿙͍͑ʢӮʣ͕ͳ͍͜ͱΛ֬ೝͨ͠‫ޙ‬ɼঃʑʹϘϯϕͷ݁߹‫ܧ‬ 20 K 2436ɿ2007 खΛ؇ΊɼϘϯϕΛऔΓ֎͠ɼόΠύε‫ͼٴ‬Ϙϯϕͷ‫ܧ‬ख෦෼ʹ෇ண͍ͯ͠ΔӷΛɼ෍ͳͲΛ༻͍ ͯ;͖औΔɻ 5) όΠύεϥΠϯʹަ‫༻׵‬ϘϯϕΛऔΓ෇͚Δ͔ຢ͸औ෇͚෦ʹΩϟοϓͳͲΛऔΓ෇͚Δɻ 6) ࢼྉΛϘϯϕ͔Βࢼྉ༰‫ʹث‬Ҡ͠ೖΕΔɻ A.2.2.4 ϕϯθϯɼϑΣϊʔϧͳͲ͕‫ͨ͠ݻڽ‬৔߹͸ɼͳΔ΂͘௿ԹͰ༥ղ͠ɼ‫׬‬શʹӷঢ়ͱͨ͠‫ޙ‬ɼ࠾ औ͢Δɻ A.2.2.5 ୅දࢼྉ͸ɼࢼྉ༰‫ʹث‬ೖΕີખͯ͠อଘ͠ɼࢼ‫͍༻ʹݧ‬Δɻ A.3 ‫ݻ‬ମࢼྉ࠾औํ๏ A.3.1 ‫۩ث‬ A.3.1.1 αϯϓϦϯάείοϓç ྫΛਤ A.6 ʹࣔ͢ɻੇ๏͸దٓͷ΋ͷͰΑ͍ɻ ਤ A.6ʵαϯϓϦϯάείοϓͷྫ A.3.1.2 ॖ෼‫ث‬ç ྫΛਤ A.7 ʹࣔ͢ɻ ਤ A.7ʵॖ෼‫ث‬ͷྫ A.3.2 ૢ࡞ A.3.2.1 খ‫ܗ‬༰‫ث‬ͷ৔߹ ද A.2 ʹΑͬͯൈ͖औ֤ͬͨ༰‫͔ث‬Β 200ʙ300 g ͷ΄΅ҰఆྔͷࢼྉΛ࠾औͯࠞ͠߹͠ɼߋʹ֤༰‫ث‬ͷ ࢼྉΛಉྔͣͭࠞ߹͠ɼ10 mm ҎԼʹคࡅͯ͠े෼ʹࠞ߹͠ɼJIS M 8100 ͷ 6.5.2ʢΠϯΫϦϝϯτॖ෼ํ ๏ʣຢ͸ॖ෼‫ث‬Λ༻͍ͯ 1 kg Ҏ্·Ͱॖ෼ͨ͠΋ͷΛɼ୅දࢼྉͱ͢Δɻ A.3.2.2 େ‫ܗ‬༰‫ث‬ͷ৔߹ 21 K 2436ɿ2007 ௨ৗ͸ɼੵࠐΈதɼडೖΕதɼ෷ग़͠தຢ͸ՙԼΖ͠தʹɼ༰қʹ࠾औͰ͖Δ৔ॴʹ͓͍ͯɼϩοτͷ ࣭ྔΛ౳෼͢ΔΑ͏ͳִؒΛ͓͍ͯɼϩοτશମͷ໿ 1 000 ෼ͷ 1 ͷ࣭ྔʢͨͩ͠ɼ100 kg Λ௒͑ͳ͍࣭ ྔʣͷࢼྉΛ໿ 1 kg ͣͭ࠾औͯࠞ͠߹͠ɼ10 mm ҎԼʹคࡅͯ͠Αࠞ͘߹͠ɼJIS M 8100 ͷ 6.5.2 ຢ͸ॖ ෼‫ث‬Λ༻͍ͯɼ1 kg Ҏ্·Ͱॖ෼ͨ͠΋ͷΛ୅දࢼྉͱ͢Δɻ ඞཁʹΑͬͯɼऩೲঢ়ଶͷ··࠾औ͢Δͱ͖΋ɼࢼྉΛͰ͖Δ͚ͩϩοτશମͷ֤෦෼͔Β࠾औ͠ɼॖ ෼ͯ͠୅දࢼྉͱ͢Δɻ A.4 ൒‫ݻ‬ମࢼྉ࠾औํ๏ A.4.1 ‫۩ث‬ ൒‫ݻ‬ମࢼྉ࠾औ‫ث‬ç ‫ܗ‬ঢ়‫ੇͼٴ‬๏ͷྫΛɼਤ A.8 ʹࣔ͢ɻ A.4.2 ૢ࡞ ༰‫ث‬ͷ‫ޱ‬Λ։͖ɼͦͷத৺෦ʹ൒‫ݻ‬ମࢼྉ࠾औ‫ث‬Λࠩ͠ࠐΈɼ‫ث‬ఈ·ͰೖΕͯࢼྉΛ࠾औ͢Δɻ ୯Ґç mm ਤ A.8ʵ൒‫ݻ‬ମࢼྉ࠾औ‫ث‬ͷྫ A.5 औѻ্͍ͷ஫ҙࣄ߲ A.5.1 อ‫۩ޢ‬ͷண༻ ໨ɼൽෘͳͲΛอ‫͢ޢ‬ΔͨΊɼద੾ͳอ‫۩ޢ‬Λண༻͢Δɻ A.5.2 ૢ࡞ ૢ࡞͸ɼ҆શΛ֬ೝ͠ͳ͕Βߦ͏ɻ 22 K 2436ɿ2007 A.5.3 ࠾औ৔ॴ ࢼྉ͔Βग़Δৠ‫ؾ‬Λ‫ٵ‬Θͳ͍Α͏ʹ෩্ʹ͓͍ͯ࠾औ͢Δɻ A.5.4 ഇ‫غ‬෺ͷॲஔ ഇ‫͢غ‬ΔࢼྉͳͲ͸ɼେ‫ؾ‬ɼਫ࣭ͷԚછ‫ͳͱݯ‬Βͳ͍Α͏ʹॲஔ͢Δɻ A.5.5 ๏‫ن‬ͷॱक ؔ࿈͢Δ๏ྩɾ๏‫ͯͬैʹن‬औΓѻΘͳ͚Ε͹ͳΒͳ͍ɻ ࢀߟจ‫ ݙ‬JIS K 2425ç ΫϨΦιʔτ༉ɾՃ޻λʔϧ‫ͼٴ‬λʔϧϐονࢼ‫ํݧ‬๏ JIS K 2435-2ç ϕϯθϯɾτϧΤϯɾΩγϨϯʵୈ 2 ෦ɿτϧΤϯ JIS K 2435-3ç ϕϯθϯɾτϧΤϯɾΩγϨϯʵୈ 3 ෦ɿΩγϨϯ JIS K 2437ç ϑΣϊʔϧྨʢϑΣϊʔϧɾΫϨκʔϧ‫ͼٴ‬ΫϨκʔϧࢎɾΩγϨϊʔϧࢎʣ JIS K 2438ç ϐϦδϯྨʢϐϦδϯɾϐίϦϯɾΩϊϦϯʣ JIS K 2439ç ΫϨΦιʔτ༉ɾՃ޻λʔϧɾλʔϧϐον ISO 1995:1981ç Aromatic hydrocarbonsʵSampling ISO 3165:1976ç Sampling of chemical products for industrial useʵSafety in sampling ISO 3170:2004ç Petroleum liquidsʵManual sampling ISO 3171:1988ç Petroleum liquidsʵAutomatic pipeline sampling

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